HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → NSC210282
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 3-Chloro-4-hydroxybenzoic acid | HCID 19860 | — |
| Product | NSC210282 | HCID 308481 | 55.5% |
Reaction Steps
Using 3-chloro-4-hydroxybenzoic acid 1/2 hydrate (25 g, 0.14 mole) and benzyl chloride (52.3 g, 0.41 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1) to give 20.4 g of 4-benzyloxy-3-chlorobenzoic acid as white crystals having a m.p. of 211°-213° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05677112 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-f06f140a9b3b4f918c9152e15f979ee5 |
| Source note | uspto-grants-1997_10 |