HCID 9842025, compound → HCID 21782804, compound

HRID 1489009Notes

Reaction equation

HRID 1489009 reaction equation
[Cl:1][C:2]1[CH:26]=[CH:25][C:5]2[O:6][C:7]3[CH:24]=[CH:23][CH:22]=[CH:21][C:8]=3[C@@H:9]3[C@H:13]([C:14]4[CH:19]=[CH:18][N:17]=[CH:16][CH:15]=4)[O:12][C:11](=[O:20])[N:10]3[C:4]=2[CH:3]=1>O>[Cl:1][C:2]1[CH:26]=[CH:25][C:5]2[O:6][C:7]3[CH:24]=[CH:23][CH:22]=[CH:21][C:8]=3[C@H:9]3[C@H:13]([C:14]4[CH:15]=[CH:16][N:17]=[CH:18][CH:19]=4)[O:12][C:11](=[O:20])[N:10]3[C:4]=2[CH:3]=1

Participants

3

Reactant 1

HCID 9842025HCID 9842025, compound

Product 1

HCID 21782804HCID 21782804, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

(-)-trans-6-chloro-1,13b-dihydro-1-(4-pyridyl)-3H-dibenz[b,f]oxazolo[3,4-d][1,4]oxazepin-3-one 6b specific rotation -50.2° @ 589 nM; Analysis Calculated for C20H13N2O3Cl×1.5 H2O: C, 61.31; H, 4.12; N, 7.15. Found: C, 61.38; H, 4.13; N, 6.82.

Sources & evidence

ORD record
ord-c60e7a0d5e454fe8adea7db84ac4c0bf
Source dataset
uspto-grants-1997_10
Patent number
US05677296

Reaction notes

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