HCID 21458444, compound → HCID 21458453, compound

Participants

Reaction Steps

A 100 mL Autoclave pressure reactor was charged with 9.2 g (8.3 mmol) of 8, 50 mL of ethanol and 3 g of 10% Pd/C. The reactor was pressurized to 220 psig with hydrogen for 3 hours at 80° C. The mixture was filtered and the filtrate was concentrated to a slightly yellow oil. 1H NMR, 13C NMR, and mass spectroscopy data were consistent with 9. The yield of 9 was essentially quantitative.

Provenance & Evidence