Toluene → HCID 86751423, compound

Participants

Reaction Conditions

Reaction Steps

231 g (1 mol) of ethyl 1-benzyl-2,5-dihydropyrrole-3-carboxylate and 10 g of 4-tert-butylpyrocatechol are dissolved in 1500 ml of toluene, 20 bar of nitrogen are injected and 350 g of 1,3-betadiene are then blown into the autoclave. The mixture is heated at 120° C. for three days and cooled, the pressure is released, and the solution is concentrated and distilled. Yield: 264.9 g (87.6% of theory), boiling point: 127°-140° C./0.1 mbar. The product is 94% pure according to gas-chromatographic detemination.

Provenance & Evidence