HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methoxyacetyl-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamin → N-(2-methoxyethyl)-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methoxyacetyl-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamin | HCID 19705334 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | N-(2-methoxyethyl)-2-(3,4-dichlorophenyl)-4-(tetrahydropyran-2-yloxy)butylamine | HCID 19705336 | — |
Reaction Steps
A suspension of 1.5 g of LiA1H4 in 30 ml of tetrahydrofuran (THF) is refluxed and a solution of 7.5 g of the product obtained in step 1 in 40 ml of THF are added dropwise thereto.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05679693 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-9aaafc3402c5458eaf4a8bf4d172101a |
| Source note | uspto-grants-1997_10 |