HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Bromide → Methyl 3-acetyl-4-(benzyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Bromide | HCID 7498 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Methyl 3-acetyl-4-hydroxybenzoate | HCID 12332833 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Methyl 3-acetyl-4-(benzyloxy)benzoate | HCID 22101033 | — |
Reaction Steps
1.0 eq. of methyl 3-acetyl-4-hydroxybenzoate was reacted with 1.1 eq. each of K2CO3 and benzyl bromide in absolute DMF to form methyl 3-acetyl-4-benzyloxybenzoate. Colorless crystals, mp 68°-72° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05679712 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-f29a42dab28e4cd0a3aea05c0a2a0e36 |
| Source note | uspto-grants-1997_10 |