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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1489801Generated: October 30, 2026

N-bromobutanimide → Methyl 3-acetyl-5-bromo-4-hydroxybenzoate

https://huagongshe.com/reaction/1489801

Reaction equation

Participants

RoleNameHCIDCharge
ReactantN-bromobutanimideHCID 67184—
ReactantMethyl 3-acetyl-4-hydroxybenzoateHCID 12332833—
SolventChlorobenzeneHCID 7964—
ProductMethyl 3-acetyl-5-bromo-4-hydroxybenzoateHCID 15818980—

Reaction Steps

Methyl 3-acetyl-4-hydroxybenzoate was reacted in chlorobenzene with 1.1 eq. of N-bromosuccinimide and a trace of AlBN to form methyl 3-acetyl-5-bromo-4-hydroxybenzoate. Colorless crystals, mp 106°-108° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05679712
Source datasetuspto-grants-1997_10
ORD IDord-232bd333759b432bada76dc1e04aaa22
Source noteuspto-grants-1997_10