Acrylic Acid → Trichlorogermylpropionic acid

HRID 1489827Notes

Reaction equation

[Cl:1][GeH:2]([Cl:4])[Cl:3].[C:5]([OH:9])(=[O:8])[CH:6]=[CH2:7]>>[Cl:1][Ge:2]([CH:6]([CH3:7])[C:5]([OH:9])=[O:8])([Cl:4])[Cl:3]

Participants

Reactant 2

HCID 6581Acrylic Acid

HCID 70900CID 70900

Product 1

HCID 13587901Trichlorogermylpropionic acid

Procedure

Trichlorogermane (Cl3GeH) was added to acrylic acid (CH2CHCOOH) to obtain trichlorogermylpropionic acid (Cl3GeCH2CH2 COOH). It was hydrolyzed to synthesize an organogermanium compound (1). In the same manner were synthesized organogermanium compounds (2) to (51).

Sources & evidence

ORD record: ord-475a9231fe514e16b33ca026b4a3a09a
Source dataset: uspto-grants-1997_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05679787

Reaction notes

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