HuagongsheHuagongshe Chemistry Print Report · For research reference only
Copper iodide → HCID 178491782, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Copper iodide | HCID 83717 | — |
| Reactant | 4-Ethynyl-1,2-dimethoxybenzene | HCID 3616421 | — |
| Solvent | Ammonia | HCID 222 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178491782 | HCID 178491782 | 48.1% |
Reaction Steps
In 15 ml of aqueous ammonia was dissolved 0.39 g of copper iodide, and the solution was added to a solution of 0.33 g of 3,4-dimethoxyphenylacetylene in 20 ml of ethanol at room temperature. The mixture was stirred for 1 hour, filtered, washed five times with water, once with ethanol, and once with ethyl ether, and dried under reduced pressure at 40° C. to yield 110 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05681954 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-5ec17252439b4e45bad9a2ec66ba954b |
| Source note | uspto-grants-1997_10 |