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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1490334Generated: October 31, 2026

Copper iodide → HCID 178491782, compound

https://huagongshe.com/reaction/1490334

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCopper iodideHCID 83717—
Reactant4-Ethynyl-1,2-dimethoxybenzeneHCID 3616421—
SolventAmmoniaHCID 222—
SolventEthanolHCID 702—
ProductHCID 178491782HCID 17849178248.1%

Reaction Steps

In 15 ml of aqueous ammonia was dissolved 0.39 g of copper iodide, and the solution was added to a solution of 0.33 g of 3,4-dimethoxyphenylacetylene in 20 ml of ethanol at room temperature. The mixture was stirred for 1 hour, filtered, washed five times with water, once with ethanol, and once with ethyl ether, and dried under reduced pressure at 40° C. to yield 110 mg of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05681954
Source datasetuspto-grants-1997_10
ORD IDord-5ec17252439b4e45bad9a2ec66ba954b
Source noteuspto-grants-1997_10