HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobenzenesulfonyl chloride → 1-(2-(p-Chlorobenzenesulphonylamino)ethyl)naphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobenzenesulfonyl chloride | HCID 7398 | — |
| Reactant | 1-Naphthaleneethanamine | HCID 20853 | — |
| Product | 1-(2-(p-Chlorobenzenesulphonylamino)ethyl)naphthalene | HCID 15057015 | — |
Reaction Steps
Prepared from 1-(2-aminoethyl)naphthalene and 4-chlorobenzenesulphonic acid chloride analogously to Example 1a. The crude product was purified by column chromatography on silica gel using ethylene chloride/cyclohexane (2:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05681961 |
| Source dataset | uspto-grants-1997_10 |
| ORD ID | ord-62f9cfdacc90458d8e93e58f28a9b652 |
| Source note | uspto-grants-1997_10 |