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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1490614Generated: October 30, 2026

3-Methoxybenzaldehyde → 3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehyde

https://huagongshe.com/reaction/1490614

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-MethoxybenzaldehydeHCID 11569—
ReagentMethylamineHCID 6329—
Reagent3,4,7,8-Tetramethyl-1,10-phenanthrolineHCID 74265—
ReagentBis(pinacolato)diboraneHCID 2733548—
Reagent4,4,5,5-Tetramethyl[1,3,2]dioxaborolaneHCID 2734768—
CatalystBis(1,5-cyclooctadiene)dimethoxydiiridiumHCID 76001521—
SolventTetrahydrofuranHCID 8028—
Product3-Methoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzaldehydeHCID 12726369089%

Reaction Conditions

Temperature90 °C

Provenance & Evidence

DOI10.1021/jacs.5b11683
Source datasetBorylation dataset from Roche
ORD IDord-14cd34ece89e4dfd945a10e825e0f1d3
Source noteBorylation dataset from Roche