HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(tert-butoxycarbonyl)piperidine → tert-Butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(tert-butoxycarbonyl)piperidine | HCID 7010304 | — |
| Reagent | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagent | 2-Methyl-1,10-phenanthroline | HCID 4913356 | — |
| Catalyst | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Solvent | Cyclooctane | HCID 9266 | — |
| Product | tert-Butyl 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)piperidine-1-carboxylate | HCID 71700020 | 41% |
Reaction Conditions
| Temperature | 100 °C |
|---|
Provenance & Evidence
| DOI | 10.1126/science.aba6146 |
|---|---|
| Source dataset | Borylation dataset from Roche |
| ORD ID | ord-5996352a1aa340fab16b8c9d1475bbdc |
| Source note | Borylation dataset from Roche |