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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491296Generated: October 31, 2026

1,2,3-Trimethoxybenzene → 4,4,5,5-Tetramethyl-2-(3,4,5-trimethoxyphenyl)-1,3,2-dioxaborolane

https://huagongshe.com/reaction/1491296

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2,3-TrimethoxybenzeneHCID 12462—
ReagentDodecahydrotriphenyleneHCID 95278—
Reagent4,4,5,5-Tetramethyl[1,3,2]dioxaborolaneHCID 2734768—
Reagent4,4'-Di-tert-butyl-2,2'-bipyridylHCID 4249187—
CatalystBis(1,5-cyclooctadiene)dimethoxydiiridiumHCID 76001521—
SolventTetrahydrofuranHCID 8028—
Product4,4,5,5-Tetramethyl-2-(3,4,5-trimethoxyphenyl)-1,3,2-dioxaborolaneHCID 219239466%

Reaction Conditions

Temperature25 °C

Provenance & Evidence

DOI10.1021/ja400295v
Source datasetBorylation dataset from Roche
ORD IDord-7cc9fb88c2864fbb8cdf674420e7e9d7
Source noteBorylation dataset from Roche