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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491309Generated: November 1, 2026

1,2,3-Trimethoxybenzene → 4,4,5,5-Tetramethyl-2-(3,4,5-trimethoxyphenyl)-1,3,2-dioxaborolane

https://huagongshe.com/reaction/1491309

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,2,3-TrimethoxybenzeneHCID 12462—
Reagent3,4,7,8-Tetramethyl-1,10-phenanthrolineHCID 74265—
ReagentDodecahydrotriphenyleneHCID 95278—
ReagentBis(pinacolato)diboraneHCID 2733548—
CatalystBis(1,5-cyclooctadiene)dimethoxydiiridiumHCID 76001521—
SolventTetrahydrofuranHCID 8028—
Product4,4,5,5-Tetramethyl-2-(3,4,5-trimethoxyphenyl)-1,3,2-dioxaborolaneHCID 2192394688%

Reaction Conditions

Temperature80 °C

Provenance & Evidence

DOI10.1021/ja400295v
Source datasetBorylation dataset from Roche
ORD IDord-3ce2e59f8513425f8f7fb6e884050931
Source noteBorylation dataset from Roche