HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491487Generated: October 25, 2026
HCID 135074937, compound → HCID 102495452, compound
https://huagongshe.com/reaction/1491487
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 135074937 | HCID 135074937 | — |
| Reagent | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagent | 4,4,5,5-Tetramethyl[1,3,2]dioxaborolane | HCID 2734768 | — |
| Reagent | N,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazine | HCID 67601456 | — |
| Catalyst | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 102495452 | HCID 102495452 | 77% |
Reaction Steps
Following the general procedure, column chromatography (EtOAc/nhexane 1:4) afforded 9b (152 mg, 77 %) as a light yellow solid.
Provenance & Evidence
| DOI | 10.1002/anie.201104544 |
|---|
| Source dataset | Borylation dataset from Roche |
|---|
| ORD ID | ord-e4e4b0f7b3104ff184558ed7264512df |
|---|
| Source note | Borylation dataset from Roche |
|---|
