関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | HCID 141373826 | HCID 141373826 | — |
| 試薬 | Bis(pinacolato)diborane | HCID 2733548 | — |
| 試薬 | 4,4,5,5-Tetramethyl[1,3,2]dioxaborolane | HCID 2734768 | — |
| 試薬 | N,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazine | HCID 67601456 | — |
| 触媒 | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| 溶媒 | Tetrahydrofuran | HCID 8028 | — |
| 生成物 | HCID 102495449 | HCID 102495449 | 79% |
反応手順
Following the general procedure, column chromatography (EtOAc/nhexane 1:4) afforded 9c (160 mg, 79 %) as a yellow solid.
情報源と証拠
| DOI | 10.1002/anie.201104544 |
|---|
| 出典データセット | Borylation dataset from Roche |
|---|
| ORD ID | ord-0837ae1efc6d4b7fb5b2a67ee40ac839 |
|---|
| 出典メモ | Borylation dataset from Roche |
|---|
