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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491493Generated: October 31, 2026

HCID 178482852, compound → HCID 178482851, compound

https://huagongshe.com/reaction/1491493

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178482852HCID 178482852—
ReagentBis(pinacolato)diboraneHCID 2733548—
Reagent4,4,5,5-Tetramethyl[1,3,2]dioxaborolaneHCID 2734768—
ReagentN,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazineHCID 67601456—
CatalystBis(1,5-cyclooctadiene)dimethoxydiiridiumHCID 76001521—
SolventTetrahydrofuranHCID 8028—
ProductHCID 178482851HCID 17848285170%

Reaction Conditions

Temperature50 °C

Reaction Steps

Following the general procedure, column chromatography (EtOAc/nhexane 1:5) afforded 9h (131 mg, 70 %) as a yellow viscous oil.

Provenance & Evidence

DOI10.1002/anie.201104544
Source datasetBorylation dataset from Roche
ORD IDord-0ad8469d0a0143f2abf5455ccf38ca4b
Source noteBorylation dataset from Roche