HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491499Generated: October 31, 2026
HCID 168665144, compound → HCID 178484941, compound
https://huagongshe.com/reaction/1491499
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 168665144 | HCID 168665144 | — |
| Reagent | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagent | 4,4,5,5-Tetramethyl[1,3,2]dioxaborolane | HCID 2734768 | — |
| Reagent | N,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazine | HCID 67601456 | — |
| Catalyst | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178484941 | HCID 178484941 | 72% |
Reaction Steps
Following the general procedure, column chromatography in neutral alumina (EtOAc/n-hexane 1:10) afforded 11d (105 mg, 72 %) as a yellow oil.
Provenance & Evidence
| DOI | 10.1002/anie.201104544 |
|---|
| Source dataset | Borylation dataset from Roche |
|---|
| ORD ID | ord-d9d8018898024fa6bb29d3a0d7421557 |
|---|
| Source note | Borylation dataset from Roche |
|---|
