HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491502Generated: November 1, 2026
4-Chlorobenzaldehyde 2,2-dimethylhydrazone → HCID 178484938, compound
https://huagongshe.com/reaction/1491502
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chlorobenzaldehyde 2,2-dimethylhydrazone | HCID 211221 | — |
| Reagent | Bis(pinacolato)diborane | HCID 2733548 | — |
| Reagent | 4,4,5,5-Tetramethyl[1,3,2]dioxaborolane | HCID 2734768 | — |
| Reagent | N,N-Dibenzyl-N'-(pyridin-2-ylmethylene)hydrazine | HCID 67601456 | — |
| Catalyst | Bis(1,5-cyclooctadiene)dimethoxydiiridium | HCID 76001521 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178484938 | HCID 178484938 | 73% |
Reaction Steps
Following the general procedure, column chromatography in neutral alumina (EtOAc/n-hexane 1:10) afforded 11g (112 mg, 73 %).
Provenance & Evidence
| DOI | 10.1002/anie.201104544 |
|---|
| Source dataset | Borylation dataset from Roche |
|---|
| ORD ID | ord-4f76430a1a884af5b1fb0714cab85713 |
|---|
| Source note | Borylation dataset from Roche |
|---|
