HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1491511Generated: October 26, 2026
Boric Acid → 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL
https://huagongshe.com/reaction/1491511
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Boric Acid | HCID 7628 | — |
| Reactant | Hexylene Glycol | HCID 7870 | — |
| Solvent | Heptane | HCID 8900 | — |
| Product | 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL | HCID 352515 | — |
Reaction Steps
61.2 g of boric acid (1 mol) and 118.2 g of 2-methyl-2,4-pentanediol (1 mol) and 200 ml of heptane are charged to a reaction flask equipped with stirrer, Marcusson apparatus and reflux condenser. The reaction mixture is heated up to its reflux temperature (about 95° C.), with stirring, and is kept at that temperature for a 4-hour period.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05370807 |
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| Source dataset | uspto-grants-1994_12 |
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| ORD ID | ord-eaeb699ad1e74e04bbf19442810f1b08 |
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| Source note | uspto-grants-1994_12 |
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