HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyldioxirane → 1-Hydroxy-2,6-diphenyl-3,5-dimethylpiperidin-4-yl Laurate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyldioxirane | HCID 115197 | — |
| Reactant | 2,6-Diphenyl-3,5-dimethylpiperidin-4-yl Laurate | HCID 53685275 | — |
| Product | 1-Hydroxy-2,6-diphenyl-3,5-dimethylpiperidin-4-yl Laurate | HCID 53668762 | 99.5% |
Reaction Steps
The general procedure of Example 2 is repeated using 29.9 g (64.5 mmol) of 2,6-diphenyl-3,5-dimethylpiperidin-4-yl laurate and 1.24 L (64.5 mmol) of dimethyldioxirane (0.050M in acetone). 30.8 g (98% yield) of the title compound is isolated: mp 108°-112° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05371125 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-e7b9adf7f5f142d89ceee8dcc72afcdd |
| Source note | uspto-grants-1994_12 |