Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Isobutyronitrile → N-(2-morpholinophenyl)isobutyramidine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Isobutyronitrile | HCID 6559 | — |
| 반응물 | 2-Morpholinoaniline | HCID 735756 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 생성물 | N-(2-morpholinophenyl)isobutyramidine | HCID 178449872 | — |
반응 단계
A mixture of 4-(2-aminophenyl)morpholine (5.34 g), isobutyronitrile (6 g) and anhydrous aluminium chloride (12 g) was heated at 160°-170° C. for 6 hours to give N-(2-morpholinophenyl)isobutyramidine (m.p. 138° C.) which was recrystallised from a 1:1 mixture of ethylacetate and hexane.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05373008 |
| 출처 데이터셋 | uspto-grants-1994_12 |
| ORD ID | ord-dc2260a1437242ecacff361fbb87fda7 |
| 출처 메모 | uspto-grants-1994_12 |