Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Isobutyronitrile | HCID 6559 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 18952214 | HCID 18952214 | — |
| Product | HCID 178503245 | HCID 178503245 | — |
Reaction Steps
A mixture of 5-methylthio-2-morpholinoaniline (1.8 g), isobutyronitrile (1.66 g) and anhydrous aluminium chloride (3.2 g) was heated at 140° C. for 2 hours to give N-(5-methylthio-2-morpholinophenyl) isobutyramidine (m.p. 155° C.) which was recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05373008 |
|---|
| Source dataset | uspto-grants-1994_12 |
|---|
| ORD ID | ord-d23a40b0cc6b41f9b359f3479907667b |
|---|
| Source note | uspto-grants-1994_12 |
|---|
