Acrylonitrile → HCID 15746319, compound

HRID 1492190Notes

Reaction equation

HRID 1492190 reaction equation
[NH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][C:2]1=[N:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[N:14]1[CH2:19][CH2:18][O:17][CH2:16][CH2:15]1.[C:20](#[N:23])[CH:21]=[CH2:22]>>[C:20]([CH2:21][CH2:22][N:1]1[CH2:6][CH2:5][CH2:4][CH2:3][C:2]1=[N:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=1[N:14]1[CH2:15][CH2:16][O:17][CH2:18][CH2:19]1)#[N:23]

Participants

3

Reactant 2

HCID 7855AcrylonitrileHCID 178420463HCID 178420463, compound

Product 1

HCID 15746319HCID 15746319, compound

Procedure

The product of Example 1 (2.6 g) was reacted at room temperature with excess acrylonitrile (5 ml). The product was recrystallised from ethylacetate to give 4-{2-[1-(2-cyanoethyl)-2-piperidinylideneamino]phenyl}morpholine. (m.p. 148° C.).

Workup

  1. customThe product was recrystallised from ethylacetate

Sources & evidence

ORD record
ord-e67c3694cc414ff289d67d3a8f227610
Source dataset
uspto-grants-1994_12
Patent number
US05373008

Reaction notes

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