HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503978, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(2-Morpholinophenyl)thiourea | HCID 2741193 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178503978 | HCID 178503978 | — |
Reaction Steps
A solution of 1-(2-morpholinophenyl)thiourea (7.2 g) in dry methanol (30 ml) was heated at reflux with methyliodide (4.2 g) for 2 hours. The solvent was removed under reduced pressure and dry ether (15 ml) was added and on scratching gave 2-methyl-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide (m.p. 151°-152° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-cad3fee50b7346f5b53ce7976e22d40d |
| Source note | uspto-grants-1994_12 |