HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178503980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18952332 | HCID 18952332 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178503980 | HCID 178503980 | — |
Reaction Steps
A mixture of 1-(2-thiamorpholinophenyl)thiourea (12.6 g), methyl iodide (7.1 g) and acetone (60 ml) was heated at 90°-95° C. for 21/2 hours. The solvent was removed by evaporation and the residue dried under vacuum (5 mm/Hg) to give 2-methyl-1-(2-thiamorpholinophenyl)-2-thiopseudourea hydroiodide (m.p. 176°-177° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-590ddb4ce63e40beadf43e9caa4dcb17 |
| Source note | uspto-grants-1994_12 |