HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophosgene → HCID 18952326, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophosgene | HCID 10040 | — |
| Reactant | 2-Methyl-6-(1-piperidinyl)benzenamine | HCID 18952215 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 18952326 | HCID 18952326 | — |
Reaction Steps
Reaction of 6-methyl-2-piperidinoaniline (6.4 g) in dioxan (20 ml) and water (65 ml) with thiophosgene (5.7 g) at 0° C. for 30 minutes and at room temperature for 2 hours gave 6-methyl-2-piperidinophenyl isothiocyanate as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-835c75ea4c014cd28d1e512d2d4367b3 |
| Source note | uspto-grants-1994_12 |