HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 2-Methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 1-(n-Butyl)-3-(2-morpholinophenyl)thiourea | HCID 8625254 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide | HCID 18952135 | — |
Reaction Steps
A mixture of 1-(n-butyl)-3-(2-morpholinophenyl)thiourea (5.8 g) and methyliodide (3.1 g) in acetone (25 ml) was heated at reflux for 4 hours to yield 2-methyl-3-(n-butyl)-1-(2-morpholinophenyl)-2-thiopseudourea hydroiodide as a colourless solid m.p. 154°-156° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-ca5e95bd8be44316bca6fce21dc6827f |
| Source note | uspto-grants-1994_12 |