HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 18952274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | HCID 18952122 | HCID 18952122 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 18952274 | HCID 18952274 | — |
Reaction Steps
Reaction of 6-methyl-2-morpholinoaniline (8.75 g) with methyl isothiocyanate (4.7 g) in dichloromethane (50 ml) at room temperature for four days yielded N-methyl-N'-(6-methyl-2-morpholinophenyl)thiourea (m.p. 182°-183° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05373008 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-8b8036de98654f5d9f4f1fe047a87bfd |
| Source note | uspto-grants-1994_12 |