Ammonia → HCID 15746479, compound

HRID 1492288Notes

Reaction equation

HRID 1492288 reaction equation
[CH3:1][C:2]1[C:3]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[C:4]([N:8]=[C:9]=[S:10])[CH:5]=[CH:6][CH:7]=1.[NH3:17]>C(O)C>[CH3:1][C:2]1[C:3]([N:11]2[CH2:16][CH2:15][O:14][CH2:13][CH2:12]2)=[C:4]([NH:8][C:9]([NH2:17])=[S:10])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 222AmmoniaHCID 18952287HCID 18952287, compound

Product 1

HCID 15746479HCID 15746479, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent2×

Procedure

Reaction of 3-methyl-2-morpholinophenyl isothiocyanate (8 g) in ethanol (5 ml) with a saturated solution of ammonia in ethanol (60 ml) at room temperature for 4 hours gave 1-(3-methyl-2-morpholinophenyl)thiourea (m.p. 178°-179° C.).

Sources & evidence

ORD record
ord-c40efa2bd2cf4696996f28b58662a151
Source dataset
uspto-grants-1994_12
Patent number
US05373008

Reaction notes

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