Ammonia → HCID 18952299, compound

HRID 1492292Notes

Reaction equation

HRID 1492292 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([N:9]=[C:10]=[S:11])=[C:5]([N:12]2[CH2:17][CH2:16][O:15][CH2:14][CH2:13]2)[CH:4]=1.[NH3:18]>C(O)C>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]([NH2:18])=[S:11])=[C:5]([N:12]2[CH2:17][CH2:16][O:15][CH2:14][CH2:13]2)[CH:4]=1

Participants

4

Reactant 2

HCID 222AmmoniaHCID 18952329HCID 18952329, compound

Product 1

HCID 18952299HCID 18952299, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Reaction of 4-methoxy-2-morpholinophenyl isothiocyanate (4.1 g) with a saturated solution of ammonia in ethanol (30 ml) for 24 hours at room temperature gave 1-(4-methoxy-2-morpholinophenyl)thiourea (m.p. 175° C.).

Sources & evidence

ORD record
ord-793ce67f1a154d11aa7b3ff58f5f1d2c
Source dataset
uspto-grants-1994_12
Patent number
US05373008

Reaction notes

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