Potassium Hydroxide → HCID 18952199, compound

HRID 1492293Notes

Reaction equation

HRID 1492293 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]([NH2:12])=S)=[C:5]([N:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)[CH:4]=1.O.O.O.C([O-])(=O)C.[Pb+2].C([O-])(=O)C.[OH-].[K+]>O>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([NH:9][C:10]#[N:12])=[C:5]([N:13]2[CH2:18][CH2:17][O:16][CH2:15][CH2:14]2)[CH:4]=1

Participants

5

Reactant 3

HCID 14797Potassium HydroxideHCID 22456Lead diacetate trihydrateHCID 18952299HCID 18952299, compound

Product 1

HCID 18952199HCID 18952199, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent3×

Procedure

A mixture of 1-(4-methoxy-2-morpholinophenyl)thiourea (3.8 g) suspended in water (26 ml), lead acetate trihydrate (5.7 g) in water (26 ml) and potassium hydroxide (8.4 g) in water (24 ml) was heated at 90°-95° C. for 30 minutes to give N-(4-methoxy-2-morpholinophenyl)cyanamide.

Sources & evidence

ORD record
ord-aa987b53a42742799f69ccfaf41952d1
Source dataset
uspto-grants-1994_12
Patent number
US05373008

Reaction notes

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