HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 4418042, compound → N2,N2-Diethylpyridine-2,5-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 4418042 | HCID 4418042 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | N2,N2-Diethylpyridine-2,5-diamine | HCID 11788486 | 95% |
Reaction Steps
40 g of the 2-diethylamino-5-nitropyridine was subjected to catalytic reduction in one liter of methanol through the use of 2 g of 10% Pd-C. The catalyst was removed by filtration, and the filtrate was concentrated to give 32 g of 5-amino-2-diethylaminopyridine (yield: 95%, oleaginous form).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05374601 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-03023f8f977240b196720b38354d10dc |
| Source note | uspto-grants-1994_12 |