HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1492417Generated: November 3, 2026
HCID 12571954, compound → HCID 12455099, compound
https://huagongshe.com/reaction/1492417
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 12571954 | HCID 12571954 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 12455099 | HCID 12455099 | 91.4% |
Reaction Steps
A solution of 660 mg (3.1 mmol) of N-acetyl-2-(acetylthio)-3-thiophenamine in 8 mL of toluene was degassed in a Pyrex robe under high vaccuum. The robe was subsequently sealed under high vaccuum and heated at 205° C. for 5 hr. Chromatographic separation on silica gel using hexane/EtOAc (5:1 ) gave 440 mg (80%) of the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05374635 |
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| Source dataset | uspto-grants-1994_12 |
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| ORD ID | ord-32d573b4e3ea4c7b9dd2294392dd34e2 |
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| Source note | uspto-grants-1994_12 |
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