HRID1492684

反应详情

EQUATION

反应方程式

HRID 1492684 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A mixture of elsamicin A (65.4 mg) and acetic anhydride (0.1 ml) in dry methanol (2 ml) was stirred at room temperature for 1 hour. Water (1 ml) was added and the mixture was evaporated in vacuo to give a yellow oil, which was purified by column chromatography on silica gel to give 70.5 mg (100%) of the desired product.

WORKUP

后处理

  1. customthe mixture was evaporated in vacuo
  2. customto give a yellow oil, which
  3. customwas purified by column chromatography on silica gel