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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1492689Generated: October 26, 2026

Hydrochloric Acid → 4,4-Dimethyl-5-oxohexanenitrile

https://huagongshe.com/reaction/1492689

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantAcrylonitrileHCID 7855—
Reactant3-Methyl-2-butanoneHCID 11251—
Product4,4-Dimethyl-5-oxohexanenitrileHCID 13157782—

Reaction Conditions

Temperature350 °C

Reaction Steps

A mixture of 40 g of 3-methyl-2-butanone and 2 g of Triton B was heated to 350° C., and 20 g of acrylonitrile was added to the mixture over a period of 1 hour. Then, the mixture was stirred for 18 hours, and hydrochloric acid was added to the mixture to make the mixture acidic and the mixture was extracted with ether.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05374723
Source datasetuspto-grants-1994_12
ORD IDord-4c442d135f6b46adb556341e03676ecd
Source noteuspto-grants-1994_12