HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1492689Generated: October 26, 2026
Hydrochloric Acid → 4,4-Dimethyl-5-oxohexanenitrile
https://huagongshe.com/reaction/1492689
Participants
| Role | Name | HCID | Charge |
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| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 3-Methyl-2-butanone | HCID 11251 | — |
| Product | 4,4-Dimethyl-5-oxohexanenitrile | HCID 13157782 | — |
Reaction Steps
A mixture of 40 g of 3-methyl-2-butanone and 2 g of Triton B was heated to 350° C., and 20 g of acrylonitrile was added to the mixture over a period of 1 hour. Then, the mixture was stirred for 18 hours, and hydrochloric acid was added to the mixture to make the mixture acidic and the mixture was extracted with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05374723 |
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| Source dataset | uspto-grants-1994_12 |
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| ORD ID | ord-4c442d135f6b46adb556341e03676ecd |
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| Source note | uspto-grants-1994_12 |
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