Triethylamine → HCID 15187624, compound

Participants

Reaction Steps

In an egg-plant type flask, 4,6-dimethylpyridine-2-sulfonic acid (374 mg, 2 mmol) and acetonitrile (4 ml) were charged, and then triethylamine (0.31 ml, 2.2 mmol) was added and stirred at room temperature for 1 hour. The reaction mixture was concentrated and dried under reduced pressure to obtain 4,6-dimethylpyridine-2-sulfonic acid triethylamine at a quantitative yield. Decomposition point, 270°-290° C.

Provenance & Evidence