Cyclohexanol → HCID 22406120, compound

HRID 1492731Notes

Reaction equation

HRID 1492731 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=1[NH:11][S:12]([CH3:15])(=[O:14])=[O:13].[CH:16]1([OH:22])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1>>[CH:16]1([O:22][C:2]2[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][C:3]=2[NH:11][S:12]([CH3:15])(=[O:14])=[O:13])[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17]1

Participants

3

Reactant 2

HCID 7966CyclohexanolHCID 4416401N-(2-fluoro-5-nitrophenyl)methanesulfonamide

Product 1

HCID 22406120HCID 22406120, compound

Procedure

Then, N-(2-fluoro-5-nitrophenyl)methanesulfonamide and cyclohexanol are subjected to etherification in the presence of a base to give N-(2-cyclohexyloxy-5-nitrophenyl)methanesulfonamide.

Sources & evidence

ORD record
ord-73d486dee083431cb6e3b94721fa9859
Source dataset
uspto-grants-1994_12
Patent number
US05374764

Reaction notes

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