HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 57285623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 57319918 | HCID 57319918 | — |
| Product | HCID 57285623 | HCID 57285623 | 88.4% |
Reaction Steps
The same procedure as in Reference Example 3-3 was carried out by using (2S,4R)-2-(N-benzyl-2-azetidinon-4-yl)-N-tert-butoxycarbonyl-4-tert-butyldimethylsiloxypyrrolidine diastereomer A (500 mg, 1.05 mmol) and sodium metal (75 mg, 3.26 mmol) to obtain (2S,4R)-2-(2-azetidinon-4-yl)-N-tert-butoxycarbonyl-4-tert-butyldimethylsiloxypyrrolidine diastereomer A (360 mg, yield: 88.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05374720 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-1936c808184c48cb983160334dfc07e4 |
| Source note | uspto-grants-1994_12 |