Sodium Hydroxide → HCID 18951531, compound

HRID 1492850Notes

Reaction equation

[OH-].[Na+].C[O:4][C:5](=[O:42])[C:6]1[CH:11]=[C:10]([O:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:22]=[CH:21][C:20]([O:23][CH2:24][C:25]3[CH:30]=[CH:29][CH:28]=[CH:27][CH:26]=3)=[CH:19][CH:18]=2)[CH:9]=[C:8]([O:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41])[CH:7]=1>>[CH2:32]([O:31][C:8]1[CH:7]=[C:6]([CH:11]=[C:10]([O:12][CH2:13][CH2:14][CH2:15][O:16][C:17]2[CH:18]=[CH:19][C:20]([O:23][CH2:24][C:25]3[CH:26]=[CH:27][CH:28]=[CH:29][CH:30]=3)=[CH:21][CH:22]=2)[CH:9]=1)[C:5]([OH:42])=[O:4])[CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH2:38][CH2:39][CH2:40][CH3:41]

Participants

Reactant 2

HCID 14798Sodium Hydroxide

HCID 54244235HCID 54244235, compound

Product 1

HCID 18951531HCID 18951531, compoundYield 95%

Procedure

Sodium hydroxide hydrolysis of 3-(decyloxy)-5-[3-[4-(phenylmethoxy)phenoxy]propoxy]benzoic acid methyl ester gave 3-(decyloxy)-5-[3-[4-(phenylmethoxy)phenoxy]propoxy]benzoic acid (95% yield, mp 107°-109°)

Sources & evidence

ORD record: ord-99de593fec6743f6a03b725ebbb2b31f
Source dataset: uspto-grants-1994_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05374772

Reaction notes

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