HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → 2-dodecylthio-N-(salicylidene)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | 2-(Dodecylthio)-aniline | HCID 4670379 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 2-dodecylthio-N-(salicylidene)aniline | HCID 136084610 | 97.2% |
Reaction Steps
Into a 1-liter flask equipped with condenser, stirrer and thermometer, were placed 220 g (0.75 mol of 2-(dodecylthio)aniline, 200 g of ethanol, and 91.5 g (0.75 mol) of salicylaldehyde. The resultant solution was heated at reflux overnight. Upon cooling, solvent was removed at reduced pressure to afford 290 g (97%) of product as a dark yellow/brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05376451 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-e376a7c11818497e9a92e5656d2c5768 |
| Source note | uspto-grants-1994_12 |