HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 780187, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | 4-[(4-chlorobenzyl)oxy]benzoic acid | HCID 961608 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 780187 | HCID 780187 | — |
Reaction Steps
2.75 mol of hydrazine hydrate was added to a solution of 0.275 mol of ethyl ester of 4-(4-chloro benzyloxy) benzoic acid (X) in 300 ml ethanol. The reaction medium was reflux-heated for 48 hours. After cooling, the expected product was separated by filtration and recrystallised from ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05376648 |
| Source dataset | uspto-grants-1994_12 |
| ORD ID | ord-e92fa0bf9ad740999afee164a641298a |
| Source note | uspto-grants-1994_12 |