Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 23720268 | HCID 23720268 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19969063 | HCID 19969063 | — |
Reaction Steps
To a solution of thionyl chloride (0.692 ml) and N,N-dimethylformamide (0.022 ml) was added sodium 6-octyloxy-2-naphthalenesulfonate (1 g) under ice-cooling and stirred for 1.5 hours at 95° C. The reaction mixture was evaporated under reduced pressure to give 6-octyloxy-2-naphthylsulfonyl chloride (1 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05376634 |
|---|
| Source dataset | uspto-grants-1994_12 |
|---|
| ORD ID | ord-8dfe9bd665274b97bd1eeb6a7b2ab5bd |
|---|
| Source note | uspto-grants-1994_12 |
|---|
