HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19830594, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 4-tert-Butylphenol | HCID 7393 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-(4-chloro-3-nitrophenyl)methanesulfonamide | HCID 3755760 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | HCID 19830594 | HCID 19830594 | — |
Reaction Steps
N-(4-chloro-3-nitrophenyl)methanesulphonamide (50 g, 0.2 mole), 4-t-butylphenol (33 g, 0.22 mole), potassium carbonate (62.1 g, 0.45 mole) and diglyme (50 ml) were heated and stirred at 165°-170° for 24 hr. The mixture was cooled to 110° and xylene (150 ml) followed by a mixture of 10M-hydrochloric acid (55 ml) and water (130 ml) added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05021333 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-ae428aa6bb0d4d399b66e410cbcd4fe2 |
| Source note | uspto-grants-1991_06 |