HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine → HCID 178483217, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(3-Aminopropoxy)-N,N-dimethylbenzenemethanamine | HCID 12913950 | — |
| Reactant | N-Nitro-S-methylisothiourea | HCID 135927615 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178483217 | HCID 178483217 | — |
Reaction Steps
N-nitrocarbamimidothioic acid methylester (0.77 g) and 3-(3-aminopropoxy)-N,N-dimethylbenzenemethanamine (1.0 g) were heated in ethanol at 40° for 20 mins. The solution was cooled to precipitate the title compound which was filtered off and recrystallised from ethyl acetate as a white solid (0.44 g) m.p. 114°-115°. TLC silica; methanol:0.88 ammonia (80:1) Rf 0.48.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05021429 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-d2184bac8fa548eaa0cc7383d0fcedfd |
| Source note | uspto-grants-1991_06 |