Ammonium Chloride → HCID 178454967, compound

HRID 1493341Notes

Reaction equation

HRID 1493341 reaction equation
N1C=[C:4]([CH2:6][CH2:7][CH2:8][NH:9][C:10]([NH:12][CH:13]([CH2:23][CH3:24])[CH2:14][S:15][CH2:16][C:17]2[N:18]=[CH:19][NH:20][C:21]=2[CH3:22])=[NH:11])[N:3]=[CH:2]1.[C:25](NC(N)=N)#[N:26].[Cl-:31].[NH4+]>>[ClH:31].[ClH:31].[ClH:31].[NH:3]1[CH:2]=[CH:25][N:26]=[C:4]1[CH2:6][CH2:7][CH2:8][NH:9][C:10]([NH:12][CH:13]([CH2:23][CH3:24])[CH2:14][S:15][CH2:16][C:17]1[N:18]=[CH:19][NH:20][C:21]=1[CH3:22])=[NH:11]

Participants

4

Reactant 3

HCID 25517Ammonium ChlorideHCID 178418324HCID 178418324, compoundHCID 178454966HCID 178454966, compound

Product 1

HCID 178454967HCID 178454967, compound

Procedure

N-[3-(Imidazol-4-yl)propyl]-N'-[1-[(5-methylimidazol-4-yl) methylthio]2-butyl]-guanidine ##STR103## prepared by a method analogous to that of Example 39 from 0.71 g (1.9 mmol) of the previously prepared cyanoguanidine. 0.97 g of a hygroscopic foam composed of equimolar quantities of ammonium chloride and N-[3-(imidazol--yl)propyl]-N'-[1-[(5-methylimidazol-4-yl)methylthio]-2-butyl]-guanidine trihydrochloride is obtained as residue.

Sources & evidence

ORD record
ord-508b382250584a5b91e8336c8ef46d75
Source dataset
uspto-grants-1991_06
Patent number
US05021431

Reaction notes

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