2,3-Dihydroxybutanedioic Acid → HCID 86744821, compound

HRID 1493354Notes

Reaction equation

HRID 1493354 reaction equation
[NH2:1][CH2:2][CH:3]1[CH2:7][CH2:6][CH2:5][N:4]1[CH2:8][CH3:9].C(O)(=O)C(C(C(O)=O)O)O>C(Cl)(Cl)Cl>[NH2:1][CH2:2][CH:3]1[CH2:7][CH2:6][CH2:5][N:4]1[CH2:8][CH3:9].[NH2:1][CH2:2][CH:3]1[CH2:7][CH2:6][CH2:5][N:4]1[CH2:8][CH3:9]

Participants

4

Reactant 2

HCID 8752,3-Dihydroxybutanedioic AcidHCID 1172952-Aminomethyl-1-ethylpyrrolidine

Product 1

HCID 86744821HCID 86744821, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

(-)2-Aminomethyl-1-ethylpyrrolidine was similarly prepared using D(-) tartaric acid as resolving agent. b15 ~62° (9.4 g) (α)58925 =-151° (50% chloroform).

Sources & evidence

ORD record
ord-d57b6d9b4dff42669a14a9071f925bdf
Source dataset
uspto-grants-1991_06
Patent number
US05021449

Reaction notes

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