2,4,8,10-Tetraoxa-3,9-diphosphaspiro[5.5]undecane, 3,9-dichloro- → HCID 57679226, compound

HRID 1493405Notes

Reaction equation

HRID 1493405 reaction equation
[CH:1]1([O:7][N:8]2[C:13]([CH3:15])([CH3:14])[CH2:12][CH:11]([NH:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[CH2:10][C:9]2([CH3:30])[CH3:29])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.Cl[P:32]1[O:37][CH2:36][C:35]2([CH2:42][O:41][P:40](Cl)[O:39][CH2:38]2)[CH2:34][O:33]1>>[CH:1]1([O:7][N:8]2[C:9]([CH3:29])([CH3:30])[CH2:10][CH:11]([N:16]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[P:32]3[O:37][CH2:36][C:35]4([CH2:42][O:41][P:40]([N:16]([CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH3:28])[CH:11]5[CH2:12][C:13]([CH3:14])([CH3:15])[N:8]([O:7][CH:1]6[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]6)[C:9]([CH3:29])([CH3:30])[CH2:10]5)[O:39][CH2:38]4)[CH2:34][O:33]3)[CH2:12][C:13]2([CH3:14])[CH3:15])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]1

Participants

3

Reactant 2

HCID 772022,4,8,10-Tetraoxa-3,9-diphosphaspiro[5.5]undecane, 3,9-dichloro-HCID 19768347HCID 19768347, compound

Product 1

HCID 57679226HCID 57679226, compound

Procedure

The title compound is prepared as a viscous oil from 1-cyclohexyloxy-4-dodecylamino-2,2,6,6-tetramethylpiperidine (made in Example 12A) and 3,9-dichloro-2,4,8,10-tetraoxa-3, 9-diphosphaspiro-[5.5]undecane according to the procedure of Example 14.

Sources & evidence

ORD record
ord-c99a232d51e24740aef5efe044841112
Source dataset
uspto-grants-1991_06
Patent number
US05021481

Reaction notes

Loading…