Benzylamine → HCID 14613353, compound

HRID 1493504Notes

Reaction equation

HRID 1493504 reaction equation
[CH3:1][C:2](Cl)([C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=[CH2:9])[C:3]([O:5]CC)=O.[CH2:17]([NH2:24])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>>[CH2:17]([N:24]1[CH2:9][C:8]([C:10]2[CH:11]=[CH:12][CH:13]=[CH:14][CH:15]=2)=[C:2]([CH3:1])[C:3]1=[O:5])[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 7504BenzylamineHCID 10900709HCID 10900709, compound

Product 1

HCID 14613353HCID 14613353, compound

Procedure

Generally following the procedures of the preceding examples, ethyl 2-methyl-2-chloro-3-phenyl-3-butenoate (R=phenyl, R1 =methyl) was reacted with benzylamine to yield N-benzyl-3-methyl-4-phenyl-3-azoline-2-one (R=phenyl, R1 =methyl).

Sources & evidence

ORD record
ord-bcbe7d7cf0874586856862b701bbc3cc
Source dataset
uspto-grants-1991_06
Patent number
US05021587

Reaction notes

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