HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86742621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sulfamic Acid | HCID 5987 | — |
| Reactant | Mannitol | HCID 6251 | — |
| Reactant | Pyrrole | HCID 8027 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86742621 | HCID 86742621 | — |
Reaction Steps
Mannityl hexasulfate ammonium salt is prepared from mannitol and sulfamic acid in dimethylformamide. A mixture of 5 grams of pyrrole and 1 gram of this ammonium salt is dissolved in 200 ml. of water. Utilizing the apparatus described in Example 7, the polymerization is carried out at a current of about 0.4 amperes over a period of 20 minutes. The product is a black electronically conducting film which is shiny on the substrate side and rough on the solution side.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05023133 |
| Source dataset | uspto-grants-1991_06 |
| ORD ID | ord-026d1907345149cbb8e6a417c3f1005c |
| Source note | uspto-grants-1991_06 |